Handbook of Sample Preparation

JANUSZ PAWLISZYN, PhD, is a Professor in the Department of Chemistry at the University of Waterloo in Ontario, Canada. He is the author of Solid Phase Microextraction (Wiley) and Sampling and Sample Preparation in Field and Laboratory, and has been published in more than four hundred scientific publications. HEATHER L. LORD, PhD, is a Research Associate for New Analytical Methods and Technologies in the Department of Chemistry at the University of Waterloo. She received her PhD in 2005 under Dr. Pawliszyn.

• Preface viiContributors ixPart I Fundamental Extraction Techniques 11 Theory of Extraction 3Janusz Pawliszyn2 Headspace Gas Chromatography 25Zelda E. Penton3 Liquid–Liquid Extraction in Environmental Analysis 39Toh Ming Hii and Hian Kee Lee4 Solid-Phase Extraction 53Ronald E. Majors5 Solid-Phase Microextraction 81Sanja Risticevic, Dajana Vuckovic, and Janusz Pawliszyn6 Microdialysis Sampling as a Sample Preparation Method 103Pradyot Nandi and Susan M. Lunte7 Liquid-Phase Microextraction (LPME) Utilizing Porous Hollow Fibers 125Stig Pedersen-Bjergaard, Knut Einar Rasmussen, and Jan Åke Jönsson8 Sample Preparation in Membrane Introduction Mass Spectrometry 149Raimo A. Ketola, Tapio Kotiaho, and Frants R. Lauritsen9 Pressurized Fluid Extraction 163John R. Dean and Renli Ma10 Superheated Water Extraction 181Roger M. Smith11 Supercritical Fluid Extraction 191Jeremy J. Kroon and Douglas E. Raynie12 Microwave-Assisted Extraction 197J.R. Jocelyn Paré and Jacqueline M.R. Bélanger13 Chemical Derivatizations in Analytical Extractions 225Jack RosenfeldPart II Application Considerations 24714 Sample Preparation Techniques for Environmental Organic Pollutant Analysis 249Ray E. Clement and Chunyan Hao15 Sample Preparation for the Study of Flavor Compounds in Food 267Henryk H. Jeleń16 Sampling and Sample Preparation for Clinical and Pharmaceutical Analysis 285Hiroyuki Kataoka, Keita Saito, and Atsushi Yokoyama17 Statistics of Sampling and Sample Preparation 313Byron Kratochvil18 SPME Devices Integrating Sampling with Sample Preparation for On-Site Analysis 325Gangfeng OuyangPart III Recent Developments 34119 Developments in the Use of Passive Sampling Devices for Monitoring Pollutants in Water 343Graham A. Mills, Rocio Aguilar-Martínez, Richard Greenwood, Ian J. Allan, Janine Brümmer, Jesper Knutsson, and Branislav Vrana20 Solid-Phase Microextraction for Drug Analysis 365Heather L. Lord21 Sample Handling Protocols for Biosensor Applications 385Andrew Chan, Teresa Artuso, and Ulrich J. Krull22 Sol-Gel Coatings and Monoliths in Analytical Sample Preparation 419Scott Segro and Abdul Malik23 The Use of Molecularly Imprinted Polymers for Sampling and Sample Preparation 445Börje Sellergren and Antonio Martin EstebanIndex 475

“Handbook of Sample Preparation" is a valuable book dealing with a wide range of state-of-the-art extraction techniques that have been used in many laboratories. Not only a good text book on a variety of extraction techniques, it also enables systematic understanding of the modern sample-preparation methods necessary for workers dealing with the analysis of various complex mixtures.”  (Anal Bioanal Chem, 2011)