Battery Materials Characterization

Advanced Techniques and Applications

Inbunden, Engelska, 2026

1 939 kr

Kommande

Connect battery materials properties to performance through advanced characterization techniques Understanding electrochemical processes during battery cycling demands specialized analytical tools that go beyond static analysis. Battery Materials Characterization: Advanced Techniques and Applications, written by two searchers with combined publications exceeding 280 papers in energy materials and synchrotron radiation, covers a wide range of battery types and the in situ/operando characterization methods required to link materials properties with electrochemical performance. The book provides dedicated treatment of XAS, TXM, ND/PDF, RIXS, EPR, TOF-SIMS, DEMS, and Cs-TEM variants applied to battery systems. Each technique is examined through case studies addressing material degradation, interfacial reactions, dynamic structural evolution, and electronic state changes under operational conditions. Coverage extends to multimodal analysis approaches that combine multiple methods for multiscale, multidimensional characterization of battery materials. The book also covers: In situ and operando characterization methods enabling real-time tracking of material dynamics during battery cycling and operationIntegration of multi-mode characterizations combining spectroscopy, microscopy, and diffraction for multiscale analysis of electrode materialsActionable guidance and real-world case studies demonstrating practical application of each analytical technique to battery researchMachine learning and large-scale data analysis approaches applied to characterization data interpretation and materials discoveryEmerging ultrafast and high-resolution methods representing future directions in battery materials analysis and electrochemical researchWritten for materials scientists, electrochemists, spectroscopists, structural chemists, solid state chemists, and physical chemists, this reference connects advanced characterization techniques with practical battery research applications. It serves researchers and practitioners who require authoritative, technique-specific guidance across multiple battery chemistries and analytical methods.

Produktinformation

Utgivningsdatum2026-09-02
Mått170 x 244 x undefined mm
FormatInbunden
SpråkEngelska
Antal sidor384
FörlagWiley-VCH Verlag GmbH
ISBN9783527355785

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Ning Li is an associate professor at Beijing Institute of Technology and sub-platform leader and head of new energy technology at BIT Chongqing Innovation Center. He conducted postdoctoral research at Lawrence Berkeley National Laboratory focusing on energy materials including silicon-based anodes, layered cathodes, and synchrotron radiation characterization. Liang Zhang is a full professor at FUNSOM at Soochow University. His research focuses on energy storage materials and synchrotron radiation, including in situ/operando X-ray spectroscopy (XAS/XES/RIXS/XPS) and the development of new synchrotron radiation-based spectroscopy and microscopy methods for energy storage and conversion materials.

About the Author ixPreface xi1 Fundamentals of Battery Materials and the Evolution of Advanced Characterization Techniques 11.1 Global Energy Transition 11.2 Basic Principles and Core Composition of Lithium-Ion Batteries 31.3 Development Trend and Core Characteristics of Secondary Batteries 71.4 Research Trend and Core Bottlenecks of Key Battery Components 111.5 Evolution of Characterization Technology 142 Neutron Scattering and Pair Distribution Function Analysis for Battery Materials 192.1 Introduction 192.2 Neutron Facilities: Global Distribution and Specialized Capabilities 212.3 Fundamental Comparison: Neutrons vs. Electrons vs. X-rays for Material Characterization 302.4 Neutron Scattering Techniques: Principles and Variants 322.5 Applications of Neutron Techniques in Energy Storage Materials 402.6 Challenges and Future Directions 493 X-ray Diffraction and Scattering Techniques: From Crystal Structure to Multiscale Structural Analysis 553.1 Fundamentals and Techniques of X-ray Diffraction 553.2 Synchrotron Radiation XRD 673.3 Small-angle/Wide-angle X-ray Scattering Techniques 723.4 Application Cases 773.5 Conclusions and Perspectives 894 Transmission Electron Microscopy for Atomic Scale and Dynamic Characterization of Battery Materials 954.1 Electron Beam Imaging and Basic Configuration of Transmission Electron Microscopy (TEM) 954.2 Electron Diffraction 1004.3 Different Imaging Modes and Contrast Imaging 1054.4 Diffraction Contrast Images 1064.5 High-resolution TEM (HRTEM) Images and Phase Contrast 1084.6 STEM Images 1104.7 Introduction to New TEM Technologies 1114.8 Application Cases 1134.9 Conclusion and Prospective 1395 Transmission X-ray Microscopy for Multiphysics Imaging of Batteries 1435.1 Fundamental Principles and Theories 1435.2 Equipment and Analysis 1475.3 Introduction to Emerging TXM Technology 1585.4 Application Cases 165vi Contents5.5 Conclusion and Prospective 1796 Synchrotron-based Soft X-ray Absorption Spectroscopy for Electronic and Interfacial Characterization of Battery Materials 1856.1 Fundamentals and Theory 1856.2 Equipment and Analysis 1936.3 Application Cases 2027 Resonant Inelastic X-ray Scattering for Probing Electronic Excitations in Battery Materials 2137.1 Fundamentals and Techniques of Resonant Inelastic X-ray Scattering 2137.2 Instrumentation and Analysis of RIXS 2177.3 Application Cases 2227.4 Summary and Perspectives 2308 Synchrotron-based Hard X-ray Absorption Spectroscopy for Local Structure and Redox Chemistry in Battery Materials 2358.1 Fundamentals of Hard X-ray Absorption Spectroscopy 235Contents vii8.2 Equipment and Analysis 2468.3 Application Cases 2549 Electron Paramagnetic Resonance Spectroscopy for Defect and Redox Characterization in Battery Materials 2659.1 Basic Principles 2659.2 Equipment and Analysis 2699.3 Introduction of New Technologies 2739.4 Application Cases 2759.5 Conclusion and Prospective 28610 Raman Spectroscopic Characterization of Structural and Interfacial Evolution in Battery Materials 28910.1 Fundamental Principles and Theory 28910.2 Instrumentation and Analysis 29310.3 Advanced Techniques and In-situ Applications 29610.4 Application of Raman Spectroscopy in the Study of Battery Materials 30010.5 Summary and Outlook 32011 Gas Evolution and Surface Chemistry Analysis of Battery Materials by Differential Electrochemical Mass Spectrometry (DEMS) and Time-of-Flight Secondary Ion Mass Spectrometry (TOF-SIMS) 32311.1 Principles and Instrumentation of DEMS 32311.2 Applications of DEMS in Battery Research 33011.3 Applications of TOF-SIMS in Battery Research 34211.4 Summary and Prospects 34912 Future Directions in Advanced Characterization of Battery Materials 35512.1 In-situ Characterizations 35512.2 Multiscale and Multispectroscopic Characterizations 35812.3 Integration of Characterization and Simulation 36012.4 Artificial Intelligence in Materials Characterizations 362References 364Index 367