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The Analytical Chemistry Laboratory Companion is essential for both students and professionals, as it provides quick, clear explanations on critical topics in analytical chemistry, equipping you with the statistical tools necessary to ensure accurate and reliable data interpretation. The Analytical Chemistry Laboratory Companion serves as a reference guide for students and professionals alike who need quick explanations on specific topics, laboratory operations, the structure of designing experiments, and the use of statistics to gain increased accuracy, precision, repeatability, and reproducibility of data. This volume will also provide in-depth and advanced studies and build the necessary background knowledge for success in the field. This companion provides a concise examination of the various analytical tools used for chemistry, and defines basic analytical instrument principles, techniques, and applications in addition to exploring statistical tools useful in data interpretation, test result reporting, and common root causes for faulty data with suggested remedies. The introduction provides a concise guide on foundational topics such as developing standard operating procedures, laboratory safety, instrumental analytical methods, and common statistical tools useful for data interpretation. This companion covers both wet chemical and instrumental analysis, including their principles, applications, and pitfalls. The Analytical Chemistry Laboratory Companion is a must-have, comprehensive guide in the field of analytical chemistry.
Michael D. Holloway is President of 5th Order Industry, which provides competency development and training. He has over 38 years of industry and holds 16 professional certifications. His publications include eight authored books, numerous contributions to other books, and a patent. He is an expert in failure analysis, reliability engineering, and designed experiments for science and engineering.
Preface xxvAcknowledgement xxviiIntroduction 1Part 1: Wet Chemistry 93Titration 95Gravimetric Methods 123Precipitation Methods 141Extraction Methods 151Digestion Methods 171Colorimetric Methods 181Part 2: Instrumental Analysis 191Spectroscopy 193Chromatography 273Part 3: Thermal Analysis 449Dynamic Thermal Mechanical Analysis (DTMA) and Thermal Mechanical Analysis (TMA) 451Appendix 501Quality 551General Accounting for the Laboratory 589Review of Chemical Synthesis 667References and Review 783Index 787