Thermal Methods of Analysis

Principles, Applications and Problems

Häftad, Engelska, 1994

AvP.J. Haines,P. J. Haines,P. S. Haines,M. Reading

1 379 kr

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This text provides an introduction to those thermal methods of analysis which are established or growing in importance, with emphasis on worked examples and graded problems. Early chapters cover principles, modern instrumentation and interpretation of results, while the last section consists of case studies and problems of gradually increasing complexity. This book should be of interest to analytical chemists; physical chemists; polymer chemists; bioanalytical chemists; materials scientists; and physicists at mid-undergraduate level and in the chemical industry.

Produktinformation

Utgivningsdatum1994-12-31
Mått178 x 254 x 17 mm
Vikt569 g
FormatHäftad
SpråkEngelska
Antal sidor286
Upplaga1995
FörlagKluwer Academic Publishers Group
ISBN9780751400502

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Analytisk kemi inom Naturvetenskap och teknik

1 Introduction to thermal methods.- 1.1 Introduction.- 1.2 Historical development.- 1.3 Definitions.- 1.4 Computers and thermal methods.- 1.5 Factors affecting thermal analysis results.- 1.6 Simultaneous and complementary techniques.- 1.7 Problems.- References.- General Bibliography.- 2 Thermogravimetry.- 2.1 Introduction.- 2.2 Historical.- 2.3 Definition of thermogravimetry.- 2.4 Apparatus.- 2.5 Kinetics of reactions.- 2.6 Applications of thermogravimetry.- 2.7 Controlled rate thermogravimetry and Hi-Res• TGA.- 2.8 Problems.- References.- 3 Differential thermal analysis and differential scanning calorimetry.- 3.1 Introduction.- 3.2 Historical.- 3.3 Definitions.- 3.4 Apparatus.- 3.5 Theory of DTA and DSC.- 3.6 Heat flux DSC.- 3.7 Power-compensated DSC.- 3.8 Calibration.- 3.9 Applications.- 3.11 Problems.- References.- 4 Thermomechanical, dynamic mechanical and associated methods.- 4.1 Introduction.- 4.2 Definitions.- 4.3 Thermomechanical analysis.- 4.4 Dynamic mechanical analysis.- 4.5Dielectric thermal analysis.- 4.6 Thermally stimulated current analysis and relaxation map analysis.- 4.7 Problems.- References.- 5 Simultaneous techniques and product analysis.- 5.1 Introduction.- 5.2 Simultaneous thermal analysis.- 5.3 Evolved gas analysis.- 5.4 Detection and identification of evolved gases.- 5.5 Infrared and simultaneous TA-infrared.- 5.6 Infrared product analysis.- 5.7 Thermomicroscopy.- 5.8 X-ray methods.- 5.9 Electron microscopy and associated techniques.- 5.10 Conclusion.- 5.11 Less common thermal analysis techniques.- 5.12 Problems.- References.- 6 Problem solving and applications of thermal methods.- List of examples.- Problems/Solutions.- 6.1 Inorganic materials.- 6.2 Polymeric materials.- 6.3 Fine chemicals and pharmaceuticals.- 6.4 Other materials.- References.- Appendix: Solutions to problems in Chapters 1-5.

The book represents excellent value for money...and should be invaluable in setting examination questions or in tutorial work. A copy of the book should be available in every chemistry library. - Education in Chemistry.; ...this will probably become the standard textbook for undergraduate courses in thermal analysis. - Chemistry and Industry; This is an excellent introductory text to thermal methods of analysis, with an easily read writing style...In particular academics and students would find this text a very useful addition to their bookshelves, but it would also be useful to graduate scientists and engineers who want to find out what relevance thermal methods of analysis have to their field. - Trends in Analytical Chemistry.