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Describes the procedures for collection of samples, sample preparation, and analysis of CWC-related chemicals. It deals with analytical procedures that can be followed in well-equipped off-site laboratories (designated laboratories), as well as the on-site analytical procedures that the OPCW inspectors use in sample collection and preliminary analysis of the samples in field conditions. A one-of-a-kind, highly topical handbook for every expert in the chemical weapons fieldOutlines the methods for analysing chemical weapons both on and off siteAuthored by international experts in the field from top laboratories in both government and academic institutions
List of Contributors. Preface.Chapter 1: Introduction (Markku Mesilaakso).Chapter 2: Sampling and Analysis in the Chemical Weapons Convention and the OPCW Mobile Laboratory (Stefan Mogl).Chapter 3: On-site Analysis by the Inspection Team. Sampling, Analysis, Equipment, Procedures and Strategies (Sabine Kruger).Chapter 4: The OPCW Gas Chromatograph/Mass Spectrometer for On-site Analysis. Instrumentation, AMDIS Software and Preparations for Use (Mieczyslaw Sokolowski).Chapter 5: Hazardous Environment Monitoring (George M. Murray and David S. Lawrence).Chapter 6: A Comprehensive Review of the Official OPCW Proficiency Test (Jeanet Hendrikse).Chapter 7: The OPCW Central Analytical Database (Charles Nyanyira).Chapter 8: Analysis Strategy for Analysis of Chemicals Related to the Chemical Weapons Convention in an Off-site Laboratory (Markku Mesilaakso).Chapter 9: Sample Preparation for Analysis of Chemicals Related to the Chemical Weapons Convention in an Off-site Laboratory (Marja-Leena Kuitunen).Chapter 10: Gas Chromatography in Screening of Chemicals Related to the Chemical Weapons Convention (Olli Kostiainen).Chapter 11: Gas Chromatography/MassSpectrometry in Analysis of Chemicals Related to the Chemical Weapons Convention (Eric R. J. Wils).Chapter 12: Liquid Chromatography / Mass Spectrometry in Analysis of Chemicals Related to the Chemical Weapons Convention (R. M. Black and R. W. Read).Chapter 13: Nuclear Magnetic Resonance Spectroscopy in Analysis of Chemicals Related to the Chemical Weapons Convention (Markku Mesilaakso and Andreas Niederhauser).Chapter 14: Fourier Transform Infrared Spectroscopy in Analysis of Chemicals Related to the Chemical Weapons Convention (Martin T. Soderstrom).Chapter 15: Capillary Electrophoresis in Analysis of Chemicals Related to the Chemical Weapons Convention (Jeremy E. Melanson and Camille A. Boulet).Chapter 16: Methods for the Retrospective Detection of Exposure to Toxic Scheduled Chemicals.Part A: Analysis of Free Metabolites (R. M. Black and D. Noort).Chapter 17: Methods for Retrospective Detection of Exposure to Toxic Scheduled Chemicals.Part B: Mass Spectrometric and Immunochemical Analysis of Covalent Adducts to Proteins and DNA (D. Noort and R. M. Black).Index.
"…this book would be a significant addition to collections serving analytical and environmental chemistry research and teaching, as well as to...those interested in weapons proliferation issues." (E-STREAMS, June 2006)